<?xml version="1.0" encoding="ISO-8859-1"?><article xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance">
<front>
<journal-meta>
<journal-id>0035-001X</journal-id>
<journal-title><![CDATA[Revista mexicana de física]]></journal-title>
<abbrev-journal-title><![CDATA[Rev. mex. fis.]]></abbrev-journal-title>
<issn>0035-001X</issn>
<publisher>
<publisher-name><![CDATA[Sociedad Mexicana de Física]]></publisher-name>
</publisher>
</journal-meta>
<article-meta>
<article-id>S0035-001X2004000200017</article-id>
<title-group>
<article-title xml:lang="es"><![CDATA[Grabado anisotrópico de silicio para aplicación en micromaquinado usando plasmas de SF6/CH4/O2/Ar y SF6/CF4/O2/Ar]]></article-title>
</title-group>
<contrib-group>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Reyes-Betanzo]]></surname>
<given-names><![CDATA[C.]]></given-names>
</name>
<xref ref-type="aff" rid="A01"/>
</contrib>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Moshkalyov]]></surname>
<given-names><![CDATA[S. A.]]></given-names>
</name>
<xref ref-type="aff" rid="A02"/>
</contrib>
<contrib contrib-type="author">
<name>
<surname><![CDATA[Swart]]></surname>
<given-names><![CDATA[J.W.]]></given-names>
</name>
<xref ref-type="aff" rid="A02"/>
</contrib>
</contrib-group>
<aff id="A01">
<institution><![CDATA[,Instituto Nacional de Astrofísica, Óptica y Electrónica  ]]></institution>
<addr-line><![CDATA[Puebla ]]></addr-line>
<country>México</country>
</aff>
<aff id="A02">
<institution><![CDATA[,Universidade Estadual de Campinas Centro de Componentes Semiconductores ]]></institution>
<addr-line><![CDATA[Sao Paulo ]]></addr-line>
<country>Brasil</country>
</aff>
<pub-date pub-type="pub">
<day>00</day>
<month>00</month>
<year>2004</year>
</pub-date>
<pub-date pub-type="epub">
<day>00</day>
<month>00</month>
<year>2004</year>
</pub-date>
<volume>50</volume>
<numero>2</numero>
<fpage>203</fpage>
<lpage>207</lpage>
<copyright-statement/>
<copyright-year/>
<self-uri xlink:href="http://www.scielo.org.mx/scielo.php?script=sci_arttext&amp;pid=S0035-001X2004000200017&amp;lng=en&amp;nrm=iso"></self-uri><self-uri xlink:href="http://www.scielo.org.mx/scielo.php?script=sci_abstract&amp;pid=S0035-001X2004000200017&amp;lng=en&amp;nrm=iso"></self-uri><self-uri xlink:href="http://www.scielo.org.mx/scielo.php?script=sci_pdf&amp;pid=S0035-001X2004000200017&amp;lng=en&amp;nrm=iso"></self-uri><abstract abstract-type="short" xml:lang="es"><p><![CDATA[Investigamos el grabado iónico reactivo de silicio usando plasmas con mezclas de gases que contienen flúor SF6/CH4(CF4)/O2/Ar para su aplicación en microsistemas electromecánicos. Examinamos la velocidad de grabado y la anisotropía del perfil en función de la composición del gas, del material del electrodo y de la potencia de radio frecuencia. La profundidad de grabado se determina usando un perfilómetro y los perfiles grabados se analizan mediante un microscopio electrónico de barrido. Como material enmascarante, usamos una película de aluminio depositada por evaporación. Obtuvimos una alta anisotropía de grabado de 0.95 con profundidades de 20 a 30 micras y velocidades de grabado de aproximadamente 0.3 a 0.66 &#956;m/min. El grabado altamente anisótropo se basa en un mecanismo que aumenta el bombardeo de iones y protege las paredes por polimerización y/u oxidación para evitar el grabado lateral. Sin embargo, bajo condiciones de grabado anisótropo se observaron considerables daños en las superficies grabadas (formación de rugosidad). Para mejorar la morfología de la superficie realizamos procesos húmedos y secos de limpieza para remover los residuos superficiales producto del grabado iónico reactivo.]]></p></abstract>
<abstract abstract-type="short" xml:lang="en"><p><![CDATA[We investigated the reactive ion etching of silicon using SF6/CH4(CF4)/O2/Ar gas mixtures containing fluorine for MEMS applications. Etch rates and anisotropy of etch profiles were examined as a function of gas composition, material of electrode, and RF power. Etch depths were measured using a profilometer, and etch profiles were analyzed by scanning electron microscope. As a mask material, an aluminium film deposited by evaporation, was used. High anisotropy of etching of 0.95 was achieved at etch depths up to 20-30 micrometers and etch rates of approximately 0.3-0.6 &#956;m/min. Highly anisotropic etching is based on a mechanism that enhance the ion bombarding and protects the sidewalls due to polymerization and/or oxidation mechanisms in order to avoid the lateral etch. However, under the anisotropic etching conditions, considerable damages of the etched surfaces (roughness formation), were observed. After etching experiments, wet / dry cleaning procedures were applied to remove surface residues resulting from the reactive ion etching and to improve the etched surface morphology.]]></p></abstract>
<kwd-group>
<kwd lng="es"><![CDATA[MEMS]]></kwd>
<kwd lng="es"><![CDATA[silicio]]></kwd>
<kwd lng="es"><![CDATA[grabado profundo]]></kwd>
<kwd lng="es"><![CDATA[plasma]]></kwd>
<kwd lng="es"><![CDATA[anisotropía]]></kwd>
<kwd lng="en"><![CDATA[MEMS]]></kwd>
<kwd lng="en"><![CDATA[silicon]]></kwd>
<kwd lng="en"><![CDATA[deep etching]]></kwd>
<kwd lng="en"><![CDATA[plasma]]></kwd>
<kwd lng="en"><![CDATA[anisotropy]]></kwd>
</kwd-group>
</article-meta>
</front><body><![CDATA[  	    <p align="justify"><font face="verdana" size="4">Instrumentaci&oacute;n</font></p>  	    <p align="justify"><font face="verdana" size="2">&nbsp;</font></p>  	    <p align="center"><font face="verdana" size="4"><b>Grabado anisotr&oacute;pico de silicio para aplicaci&oacute;n en micromaquinado usando plasmas de SF<sub>6</sub>/CH<sub>4</sub>/O<sub>2</sub>/Ar y SF<sub>6</sub>/CF<sub>4</sub>/O<sub>2</sub>/Ar</b></font></p>  	    <p align="center"><font face="verdana" size="2">&nbsp;</font></p>  	    <p align="center"><font face="verdana" size="2"><b>C. Reyes&#45;Betanzo<sup>a</sup>,</b> <b>S. A. Moshkalyov<sup>b</sup> y J.W. Swart</b><b><sup>b</sup></b></font></p>  	    <p align="justify"><font face="verdana" size="2">&nbsp;</font></p>  	    <p align="justify"><font face="verdana" size="2"><sup><i>a</i></sup> <i>Instituto Nacional de Astrof&iacute;sica,</i> &Oacute;<i>ptica y Electr&oacute;nica, Apartado Postal 51 72000, Puebla, M&eacute;xico e&#45;mail</i>: <a href="mailto:creyes@inaoep.mx">creyes@inaoep.mx</a>.</font></p>  	    <p align="justify"><font face="verdana" size="2"><sup><i>b</i></sup> <i>Centro de Componentes Semiconductores, UNICAMP, 6061 CEP. 13083&#45;970, Campinas, S&atilde;o Paulo, Brasil.</i></font></p>  	    <p align="justify"><font face="verdana" size="2">&nbsp;</font></p>  	    ]]></body>
<body><![CDATA[<p align="justify"><font face="verdana" size="2">Recibido el 30 de enero de 2003.    <br> 	Aceptado el 8 de septiembre de 2003.</font></p>  	    <p align="justify"><font face="verdana" size="2">&nbsp;</font></p>  	    <p align="justify"><font face="verdana" size="2"><b>Resumen</b></font></p>  	    <p align="justify"><font face="verdana" size="2">Investigamos el grabado i&oacute;nico reactivo de silicio usando plasmas con mezclas de gases que contienen fl&uacute;or S<i>F</i><sub>6</sub><i>/</i>C<i>H</i><sub>4</sub><i>(</i>C<i>F</i><sub>4</sub>)/<i>O</i><sub>2</sub>/Ar para su aplicaci&oacute;n en microsistemas electromec&aacute;nicos. Examinamos la velocidad de grabado y la anisotrop&iacute;a del perfil en funci&oacute;n de la composici&oacute;n del gas, del material del electrodo y de la potencia de radio frecuencia. La profundidad de grabado se determina usando un perfil&oacute;metro y los perfiles grabados se analizan mediante un microscopio electr&oacute;nico de barrido. Como material enmascarante, usamos una pel&iacute;cula de aluminio depositada por evaporaci&oacute;n. Obtuvimos una alta anisotrop&iacute;a de grabado de 0.95 con profundidades de 20 a 30 micras y velocidades de grabado de aproximadamente 0.3 a 0.66 <i>&#956;</i>m/min. El grabado altamente anis&oacute;tropo se basa en un mecanismo que aumenta el bombardeo de iones y protege las paredes por polimerizaci&oacute;n y/u oxidaci&oacute;n para evitar el grabado lateral. Sin embargo, bajo condiciones de grabado anis&oacute;tropo se observaron considerables da&ntilde;os en las superficies grabadas (formaci&oacute;n de rugosidad). Para mejorar la morfolog&iacute;a de la superficie realizamos procesos h&uacute;medos y secos de limpieza para remover los residuos superficiales producto del grabado i&oacute;nico reactivo.</font></p>  	    <p align="justify"><font face="verdana" size="2"><b>Descriptores:</b> MEMS; silicio; grabado profundo; plasma; anisotrop&iacute;a.</font></p>  	    <p align="justify"><font face="verdana" size="2">&nbsp;</font></p>  	    <p align="justify"><font face="verdana" size="2"><b>Abstract</b></font></p>  	    <p align="justify"><font face="verdana" size="2">We investigated the reactive ion etching of silicon using S<i>F</i><sub>6</sub>/C<i>H</i><sub>4</sub>(C<i>F</i><sub>4</sub>)/<i>O</i><sub>2</sub>/Ar gas mixtures containing fluorine for MEMS applications. Etch rates and anisotropy of etch profiles were examined as a function of gas composition, material of electrode, and RF power. Etch depths were measured using a profilometer, and etch profiles were analyzed by scanning electron microscope. As a mask material, an aluminium film deposited by evaporation, was used. High anisotropy of etching of 0.95 was achieved at etch depths up to 20&#45;30 micrometers and etch rates of approximately 0.3&#45;0.6 <i>&#956;</i>m/min. Highly anisotropic etching is based on a mechanism that enhance the ion bombarding and protects the sidewalls due to polymerization and/or oxidation mechanisms in order to avoid the lateral etch. However, under the anisotropic etching conditions, considerable damages of the etched surfaces (roughness formation), were observed. After etching experiments, wet / dry cleaning procedures were applied to remove surface residues resulting from the reactive ion etching and to improve the etched surface morphology.</font></p>  	    <p align="justify"><font face="verdana" size="2"><b>Keywords:</b> MEMS; silicon; deep etching; plasma; anisotropy.</font></p>  	    ]]></body>
<body><![CDATA[<p align="justify"><font face="verdana" size="2">&nbsp;</font></p>  	    <p align="justify"><font face="verdana" size="2">PACS: 5275Rx; 8165cf.</font></p>  	    <p align="justify"><font face="verdana" size="2">&nbsp;</font></p>  	    <p align="justify"><font face="verdana" size="2"><a href="/pdf/rmf/v50n2/v50n2a17.pdf" target="_blank">DESCARGAR ART&Iacute;CULO EN FORMATO PDF</a></font></p>      <p align="justify"><font face="verdana" size="2">&nbsp;</font></p>  	    <p align="justify"><font face="verdana" size="2"><b>Referencias</b></font></p>  	    <!-- ref --><p align="justify"><font face="verdana" size="2">1.&nbsp;G.S. Oehrlein y Y. Kurogi, <i>Mat. Sci. Eng.</i> <b>24</b> (1998) 153.    &nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=8300298&pid=S0035-001X200400020001700001&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --></font></p>  	    <!-- ref --><p align="justify"><font face="verdana" size="2">2.&nbsp;J. Kiiham&auml;ki, H. Kattelus, J. Karttunen y S. Franssila, <i>Sens. Actuators A</i> <b>82</b> (2000) 234.    &nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;[&#160;<a href="javascript:void(0);" onclick="javascript: window.open('/scielo.php?script=sci_nlinks&ref=8300300&pid=S0035-001X200400020001700002&lng=','','width=640,height=500,resizable=yes,scrollbars=1,menubar=yes,');">Links</a>&#160;]<!-- end-ref --></font></p>  	    ]]></body>
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